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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
Section 1.4.4
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
not specified
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
N-[2-[(4-amino-m-tolyl)ethylamino]ethyl]methanesulphonamide
EC Number:
202-124-2
EC Name:
N-[2-[(4-amino-m-tolyl)ethylamino]ethyl]methanesulphonamide
Cas Number:
92-09-1
Molecular formula:
C12H21N3O2S
IUPAC Name:
N-{2-[(4-amino-3-methylphenyl)(ethyl)amino]ethyl}methanesulfonamide

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
66.5 °C
Atm. press.:
1 013 hPa
Remarks on result:
other: The melting temperature given is the average of two measurements.

Any other information on results incl. tables

Results

Measurements with the closed crucible showed a steep endothermic phase.

The endothermic signal was assigned to the following melting point: 67.35 °C / 65.72 °C (two measurements).

The average of the two values was 66.5 °C

After the heating and cooling down process a black melting remains in the crucible.

Applicant's summary and conclusion