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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
February -March 2019
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
capillary method
Key result
Melting / freezing pt.:
246.4 °C
Decomposition:
yes
Decomp. temp.:
> 246.4 - < 246.9 °C
Sublimation:
no

Replicate #

Melting Ranges Observed (°C)

Decomposition Observed (°C)

Initial[1]

Final1

Individual2

Mean ± SD

1

246.4

246.8

246.8

246.9 ± 0.1

2

246.5

246.9

246.9


[1]Test substance decomposed at 246.4 to 246.9oC. When the test temperature reached 300oC, the test substance did not melt.

[2]Decomposition was observed signaled by a color change from white to brown; therefore the test was stopped prior to melting observed.

Conclusions:
Test substance decomposed at 246.4 to 246.9oC. When the test temperature reached 300oC, the test substance did not melt
Executive summary:

Test substance decomposed at 246.4 to 246.9oC. When the test temperature reached 300oC, the test substance did not melt

Description of key information

Test substance decomposed at 246.4 to 246.9oC. When the test temperature reached 300oC, the test substance did not melt

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
246.4 °C

Additional information