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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experimental Starting Date: 29 November 2012 Experimental Completion Date: 30 November 2012
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.9 (Flash-Point)
Deviations:
no
GLP compliance:
yes
Type of method:
equilibrium method closed cup

Test material

Constituent 1
Reference substance name:
A-197
IUPAC Name:
A-197
Details on test material:
Identification: A-197
Description: pale brown liquid
Batch:B12-12212
Purity:77%
Expiry / Retest Date:20 September 2013
Storage Conditions:approximately 4 °C in the dark

Results and discussion

Flash point
Flash point:
192 °C
Atm. press.:
100.1 kPa

Any other information on results incl. tables

Results

Results of the flash point determination are shown in the following table.

 

Table 3.1

 

Temperature (ºC)

Observations

21.0

No flash.

26.0

No flash.

31.0

No flash.

36.0

No flash.

41.0

No flash.

46.0

No flash.

51.0

No flash.

56.0

No flash.

61.0

No flash.

66.0

No flash.

71.0

No flash.

71.0 (fresh sample)

No flash.

76.0

No flash.

81.0

No flash.

86.0

No flash.

91.0

No flash.

96.0

No flash.

101.0 (fresh sample)

No flash.

106.0

No flash.

111.0

No flash.

116.0

No flash.

121.0

No flash.

126.0

No flash.

131.0

No flash.

136.0

No flash.

141.0

No flash.

146.0

No flash.

151.0

No flash.

151.0 (fresh sample)

No flash.

156.0

No flash.

161.0

No flash.

166.0

No flash.

171.0

No flash.

176.0

No flash.

181.0

No flash.

186.0

No flash.

191.0

No flash.

196.0

An orange flame spread across the sample cup.

191.0 (fresh sample)

No flash.

192.0

An orange flame spread across the sample cup.

192.0 (fresh sample)

An orange flame spread across the sample cup.

192.0 (fresh sample)

An orange flame spread across the sample cup.

190.0 (fresh sample)

No flash.

190.0 (fresh sample)

No flash.

 

Atmospheric pressure =         100.1 kPa

Corrected flash point =         192.282 ºC

 

Applicant's summary and conclusion

Conclusions:
The flash point of the test item has been determined to be 192 ± 2 °C.
Executive summary:
The determination was carried out using a closed cup flash point tester[1], using a procedure designed to be compatible with Method A9 Flash Point of Commission Regulation (EC) No 440/2008 of 30 May 2008.

[1]Based on, Anon (1983) Paints, Varnishes, Petroleum and Related Products - Determination of Flash Point - Rapid Equilibrium Method,InternationalStandard ISO 3679-2004(E), Second Edition –2004-04-01, P1-18 and Anon (1989) Flash Point of Liquids by Setaflash Closed-Cup Apparatus,ASTM D-3278-89, P1-7.

Conclusion

The flash point of the test item has been determined to be 192 ± 2 °C.