5-ethyl-1,3-dioxane-5-methanol

Boiling point

Link to relevant study record(s)

Reference

Endpoint:

boiling point

Type of information:

experimental study

Adequacy of study:

key study

Study period:

2006-09-22 and 2006-12-07

Reliability:

2 (reliable with restrictions)

Rationale for reliability incl. deficiencies:

other: guideline study

Qualifier:

according to guideline

Guideline:

OECD Guideline 103 (Boiling point/boiling range)

Version / remarks:

; dynamic

Qualifier:

according to guideline

Guideline:

OECD Guideline 103 (Boiling point/boiling range)

Version / remarks:

; Distillation

Principles of method if other than guideline:

One value; dynamic
One value, distillation

GLP compliance:

no

Type of method:

distillation method

Key result

Boiling pt.:

239.5 °C

Atm. press.:

101.3 kPa

Key result

Boiling pt.:

239 °C

Atm. press.:

101.3 kPa

Decomposition:

no

The measured temperatures were corrected to 101.3 kPa at 0°C, according to ISO 918-1983 and European Pharmacopoeia 6.0 (part 2.2.11).

Value 2, distilled method

Volume	Temperature, °C
1^stdrop	237.8
1 ml	238.0
5 ml	238.3
10 ml	238.3
20 ml	238.4
30 ml	238.4
40 ml	238.4
50 ml	238.4
60 ml	238.4
70 ml	238.5
80 ml	238.5
90 ml	238.5
95 ml	238.9
Dry	239.8

Conclusions:

Boiling point: 239°C (corrected mean value from two different methods)

Executive summary:

Boiling point: 239°C (corrected mean value from two different methods)

Description of key information

Boiling point: 239°C (OECD Guideline 103, corrected mean value from both dynamic and distillation method)

Key value for chemical safety assessment

Boiling point at 101 325 Pa:

239 °C