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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP- and Guideline-Study with no or minor deficiencies.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2002

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
other: method according to Siwoloboff and differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
methyl 2-amino-5-fluorobenzoate
EC Number:
608-681-1
Cas Number:
319-24-4
Molecular formula:
C8 H8 F N O2
IUPAC Name:
methyl 2-amino-5-fluorobenzoate

Results and discussion

Boiling pointopen allclose all
Boiling pt.:
260 - 270 °C
Atm. press.:
1 013.25 hPa
Decomposition:
no
Remarks on result:
other: Method of Siwoloboff
Boiling pt.:
256 - 261 °C
Atm. press.:
1 013.25 hPa
Decomposition:
no
Remarks on result:
other: Differential scanning calorimetry

Applicant's summary and conclusion

Conclusions:
The substance has no exact boiling point. It showed a wide boiling range. For further assessments the boiling range of 260-270°C at 1013.25 hPa in which boiling was observed visually was choosen.