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EC number: 206-674-4 | CAS number: 366-18-7
- Life Cycle description
- Uses advised against
- Endpoint summary
- Appearance / physical state / colour
- Melting point / freezing point
- Boiling point
- Density
- Particle size distribution (Granulometry)
- Vapour pressure
- Partition coefficient
- Water solubility
- Solubility in organic solvents / fat solubility
- Surface tension
- Flash point
- Auto flammability
- Flammability
- Explosiveness
- Oxidising properties
- Oxidation reduction potential
- Stability in organic solvents and identity of relevant degradation products
- Storage stability and reactivity towards container material
- Stability: thermal, sunlight, metals
- pH
- Dissociation constant
- Viscosity
- Additional physico-chemical information
- Additional physico-chemical properties of nanomaterials
- Nanomaterial agglomeration / aggregation
- Nanomaterial crystalline phase
- Nanomaterial crystallite and grain size
- Nanomaterial aspect ratio / shape
- Nanomaterial specific surface area
- Nanomaterial Zeta potential
- Nanomaterial surface chemistry
- Nanomaterial dustiness
- Nanomaterial porosity
- Nanomaterial pour density
- Nanomaterial photocatalytic activity
- Nanomaterial radical formation potential
- Nanomaterial catalytic activity
- Endpoint summary
- Stability
- Biodegradation
- Bioaccumulation
- Transport and distribution
- Environmental data
- Additional information on environmental fate and behaviour
- Ecotoxicological Summary
- Aquatic toxicity
- Endpoint summary
- Short-term toxicity to fish
- Long-term toxicity to fish
- Short-term toxicity to aquatic invertebrates
- Long-term toxicity to aquatic invertebrates
- Toxicity to aquatic algae and cyanobacteria
- Toxicity to aquatic plants other than algae
- Toxicity to microorganisms
- Endocrine disrupter testing in aquatic vertebrates – in vivo
- Toxicity to other aquatic organisms
- Sediment toxicity
- Terrestrial toxicity
- Biological effects monitoring
- Biotransformation and kinetics
- Additional ecotoxological information
- Toxicological Summary
- Toxicokinetics, metabolism and distribution
- Acute Toxicity
- Irritation / corrosion
- Sensitisation
- Repeated dose toxicity
- Genetic toxicity
- Carcinogenicity
- Toxicity to reproduction
- Specific investigations
- Exposure related observations in humans
- Toxic effects on livestock and pets
- Additional toxicological data
Boiling point
Administrative data
Link to relevant study record(s)
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: According to OECD guideline 103 without deviation
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling point/boiling range)
- Deviations:
- no
- Principles of method if other than guideline:
- The above-mentioned guidelines contain several different methods for the determination of the boiling point / boiling range. These methods include thermal analysis using a calorimeter and visual tests (e.g. capillary test). During the present study the thermal analysis was used.
A phase transformation, e.g. melting or evaporation, or a reaction, e.g. dissociation, usually is associated with a heat effect. In the calorimeter, two identical aluminium sample containers, one filled with the test item and the other empty (used as a reference), are heated at a constant rate. During the experiment, the heat effect, i.e. the difference in heat flow, between the sample container and the reference container is registered.
A preliminary test was conducted in which a test item amount of 3.24 mg was heated up from 25 °C to 400 °C at a rate of 20 °C/min. The
quantities of heat absorbed or released were measured and recorded. Before and after the test, the weight and the appearance of the sample were determined.
In the main test in the temperature range investigated, a peak was observed from which boiling of the sample could be deduced, the thermal analysis was repeated in the immediate vicinity of the peak temperature with the temperature rise adjusted to 10 °C/min. For the actual determination of the boiling point, 4.63 mg and 6.81 mg, respectively, of the test item were heated up from 240 °C to 310 °C. Before and after the test, the weight and the appearance of the samples were determined. - GLP compliance:
- no
- Type of method:
- differential scanning calorimetry
- Boiling pt.:
- 272.2 °C
- Atm. press.:
- 99 kPa
- Boiling pt.:
- 545.4 K
- Atm. press.:
- 99 kPa
- Conclusions:
- The boiling point of CA3610A was determined to be 272.2 °C, which is equal to 545.4 K.
The estimated accuracy is ± 0.5 K.
This result was obtained using Differential Scanning Calorimetry (Thermal Analysis) method.
The atmospheric pressure during the measurements was 99.0 kPa.
Reference
The DSC-curve of the preliminary test (heating rate of 20 °C/min from 25 °C to 400 °C) showed a first endothermic heat effect, the melting, at about 70.8 °C (see Harlan Laboratories study D01028). A second endothermic heat effect, the boiling, was detected at about 272.8 °C. After the experiment, the sample had all of its mass and no residue remained in the sample cup.
In order to determine the boiling point more precisely, further DSC-runs were recorded between 240 °C and 310 °C with a heating rate of 10 °C/min. During these runs, the boiling point was determined to be 272.1 °C and 272.2 °C. The samples lost less than 4% of their mass, respectively. After the measurements no residue remained in the sample cups.
Description of key information
The boiling point of CA3610A was determined to be 272.2 °C (Kuehne 2010), which is equal to 545.4 K.
The estimated accuracy is ± 0.5 K.
This result was obtained using Differential Scanning Calorimetry (Thermal Analysis) method.
The atmospheric pressure during the measurements was 99.0 kPa.
Key value for chemical safety assessment
- Boiling point at 101 325 Pa:
- 272.2 °C
Additional information
A very large body of experimental data exists in the literature for boiling point. The range of boiling points observed likely reflects experimental error, as well as the larger effect of different purities. The boiling point deemed best for classification and risk assessment purposes is the key study. This is in good agreement with existing literature.
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
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