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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2004
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Acceptable, well documented company data which meets basic scientific principles.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2004
Report date:
2004

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
yes
Type of method:
capillary method

Test material

Constituent 1
Test material form:
solid: particulate/powder
Remarks:
migrated information: powder
Details on test material:
Chemical identifiers as defined in section 1.1 and 1.2.
Batch: 0374.

Results and discussion

Any other information on results incl. tables

At the conditions stepoint 40oC, gradient 10oC/min and maxpoint 390oC the preliminary melting point was determined to be 287oC.

Applicant's summary and conclusion

Conclusions:
The preliminary melting point was determined to be 287oC. At the conditions setpoint 275oC and gradient 1oC/min the precise melting
point determination of the test substance could not be performed because of thermal degradation of the test substance.
Executive summary:

The preliminary melting point was determined to be 287oC. At the conditions setpoint 275oC and gradient 1oC/min the precise melting point determination of the test substance could not be performed because of thermal degradation of the test substance.