Registration Dossier

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: ASTM method; not conducted under GLP

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2012
Report date:
2012

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: ASTM D2887
Principles of method if other than guideline:
Simulated distillation by GC is used to determine the
boiling point range of sample. Column
heating causes the sequential elution of sample
components based on their boiling point. A calibration
curve is constructed that relates carbon number and
boiling point to retention time and allows for the
determination of boiling points for the components in an
unknown test sample.
GLP compliance:
no
Type of method:
distillation method

Test material

Constituent 1
Chemical structure
Reference substance name:
Reaction mass of (6E)-2,6-dimethyl-10-methylenedodeca-2,6-diene and (6E)-3,7,11-trimethyldodeca-1,6,10-triene and (6E,10E)-2,6,10-trimethyldodeca-2,6,10-triene and (6E,10Z)-2,6,10-trimethyldodeca-2,6,10-triene
EC Number:
942-471-3
Cas Number:
1581740-29-5
Molecular formula:
C15H26
IUPAC Name:
Reaction mass of (6E)-2,6-dimethyl-10-methylenedodeca-2,6-diene and (6E)-3,7,11-trimethyldodeca-1,6,10-triene and (6E,10E)-2,6,10-trimethyldodeca-2,6,10-triene and (6E,10Z)-2,6,10-trimethyldodeca-2,6,10-triene
Details on test material:
Batch: RV-650-70-2
Sample ID: 2012-SANF-000190-028

Results and discussion

Boiling point
Boiling pt.:
> 253 °C
Atm. press.:
ca. 760 mm Hg
Decomposition:
no
Remarks on result:
other: 253 is initail biling point. Final boiling point is 303.5 C at 760 mm Hg

Any other information on results incl. tables

Initial Boiling Point = 253 C

5% recovered = 263.5 C

10% recovered = 268.0 C

15% recovered = 270.5 C

20% recovered = 273.0 C

25% recovered = 274.5 C

30% recovered = 276.5 C

35% recovered = 278.0 C

40% recovered = 279.0 C

45% recovered = 280.5 C

50% recovered = 281.5 C

55% recovered = 282.5 C

60% recovered = 284.0 C

65% recovered = 285.0 C

70% recovered = 286.0 C

75% recovered = 287.0 C

80% recovered = 287.5 C

85% recovered = 288.5 C

90% recovered = 289.5C

95% recovered = 290.0 C

Final Boiling point = 303.5 C

Applicant's summary and conclusion

Conclusions:
Initial Boiling point = 253 C at 1 atm
Final Boiliing point = 303.5 C at 1 atm
Executive summary:

Boiling point was measured using ASTM D2887, a simulated distillation protocol. Initial boiling point was 253C; Final boiling point was 303.5 C (both measured at 1 atm).