Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
1989, october 31st
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP study performed according to the Test Guidelines described in the EEC Directive 84/449/EEC.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
1989
Report date:
1989

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
yes
Type of method:
method according to Siwoloboff

Test material

Constituent 1
Chemical structure
Reference substance name:
3',5'-dichloro-4'-ethyl-2'-hydroxypalmitanilide
EC Number:
406-200-8
EC Name:
3',5'-dichloro-4'-ethyl-2'-hydroxypalmitanilide
Cas Number:
117827-06-2
Molecular formula:
C24H39Cl2NO2
IUPAC Name:
N-(3,5-dichloro-4-ethyl-2-hydroxyphenyl)hexadecanamide
Details on test material:
Identification UC—136
Description White powder
Purity 98.5%
Storage conditions At room temperature in the dark in a tightly sealed container
Stability of test substance : Stable for one year maximal under storage conditions
Safety precautions Gloves and goggies were used to assure personnel health and safety.
The test was performed in a fume cupboard.

Results and discussion

Boiling point
Boiling pt.:
ca. 423 K
Atm. press.:
101.83 kPa
Decomposition:
no

Applicant's summary and conclusion

Conclusions:
The boiling point/boiling range of UC—136 was determined using a melting
point apparatus.
During the heating process, the liquefied test substance changed gradually
from a clear practically colourless liquid into a clear brown liquid,
starting at approximately 356 K (83°C). The solid which remained after
cooling the liquid, stili had the brown colour. This indicated
decomposition and/or rearrangement.
The boiling point/boiling range of UC—136 and/or decomposition products
was determined to be at approximately 423 K (150°C).
The measurements were performed at 101.83 kPa.