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Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with generally accepted scientific standards and described in sufficient detail
Qualifier:
equivalent or similar to guideline
Guideline:
other: screening DTA (based on DIN 51007)
Deviations:
no
Principles of method if other than guideline:
Screening DTA based on DIN 51007
GLP compliance:
yes (incl. QA statement)
Type of method:
differential thermal analysis
Key result
Boiling pt.:
> 360 °C
Atm. press.:
ca. 1 atm
Decomposition:
yes

 No.  Weight (mg)  Temperature range (°C)  Type of effect  Energy (J/g)
 1  20.6

 215 -240

362 - 465

endothermic

exothermic

 

-190

 2  28.4

 215 -240

360 - 465

endothermic

exothermic

 

-190

Conclusions:
Solvent Violet 36 is a solid which decomposes before boiling.
Executive summary:

A DTA in the range of 20 to 500°C shows and endothermic process at 215 to 240°C (melting!) and an exothermic process at 360 to 465°C which can attributed to decomposition. No endothermic process attributed to boiling point can be seen.

Description of key information

Solvent Violet 36 is a solid which decomposes before boiling.

Key value for chemical safety assessment

Additional information

Thermal decomposition begins at a temperature of 360°C (method: DTA, heating rate 3 k/min) (Drafz 2018). Up to this point there is no hint for a boiling in the temperature heat/flow diagram. Solvent Violet 36 has no boiling point up to the beginning of the decomposition.