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Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
08-11-2016 – 09-11-2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental test result performed using standard test guidelines
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Principles of method if other than guideline:
The boiling point determination of Test chemicalwas done as per the test guideline OECD 103. The method followed was according to Siwoloboff.
GLP compliance:
no
Type of method:
method according to Siwoloboff
Key result
Boiling pt.:
224 °C
Atm. press.:
977.8 hPa
Decomposition:
no
Remarks on result:
other: Other details not available

Observation table & Result :

Method Details

Observations 

Remarks if, any

Guideline

OECD 103

 

 

Method

Method according to Siwoloboff

 

 

Principle of Boiling point test

A sample is heated gradually in a tube which is

immersed in a liquid bath.The sample tube is held in close contact with a thermometer and it contains

a boiling capillary which is fused about 1 cm above its lower end. Upon approach of the boiling temperature bubbles emerge rapidly from the lower open end of the capillary. The boiling temperature is that temperature at which, on momentary cooling, the

string of bubbles stops and liquid suddenly rises in the capillary.

 

 

Volume of chemical used

ml/ g

2.037 g

-

Nature of the Bath taken

·    Oil bath

·    Water bath

Oil bath

-

 

If oil bath is used, the type of oil

·    Liquid paraffin

·    Silicone oil

Silicon oil

-

Atmospheric pressure

hPa

977.8 hPa

-

Decomposition

Decomposition temperature (°C), if applicable

·                    Yes

·                    No

No

-

Boiling point (°C) (RESULT)

°C

224°C

-

Boiling point range, if applicable

°C

-

-

Conclusions:
The boiling point of test chemical 1-chloro-3-nitrobenzene is 224°C at 977.8 hPa.
Executive summary:

The boiling point determination of test chemical 1-chloro-3-nitrobenzene was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The boiling point of test chemical 1-chloro-3-nitrobenzene is 224°C at 977.8 hPa.

Description of key information

The boiling point of test chemical 1-chloro-3-nitrobenzene is 224°C at 977.8 hPa.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
224 °C

Additional information

The boiling point determination of test chemical 1-chloro-3-nitrobenzene was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The boiling point of test chemical 1-chloro-3-nitrobenzene is 224°C at 977.8 hPa.

From other reliable sources & authoritative databases boiling point of test chemical 1 -chloro-3 -nitrobenzene is in the range between 235 to 236°C.