Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

Currently viewing:

Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
July 27th, 2015
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Test conducted according to internationally accepted testing guidelines.
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Principles of method if other than guideline:
The test was performed according to the SOP - SRT 028 protocol.
GLP compliance:
no
Type of method:
differential scanning calorimetry
Decomposition:
yes
Decomp. temp.:
261 - 293 °C

The imbibition water/solvent release was observed between 50 -145 °C (onset at 59.8 °C, enthalpy: -16.2 J/g), followed by decomposition between 261 - 293 °C (onset at 264.3 °C, enthalpy 21.1 J/g).

Conclusions:
The substance decomposes before melting (261 - 293 °C)
Executive summary:
The test item melting point was determined using the Differential Scanning Calorimetry (DSC) according to Directive EC 440/2008 Method A.1., OECD Test Guideline 102 (1995).

The imbibition water/solvent release was observed between 50 -145 °C (onset at 59.8 °C, enthalpy: -16.2 J/g), followed by decomposition between 261 - 293 °C (onset at 264.3 °C, enthalpy 21.1 J/g).

Conclusion

The substance decomposes before melting (261 - 293 °C)

Description of key information

The substance decomposes before melting (261 - 293 °C)

Key value for chemical safety assessment

Additional information

Differential Scanning Calorimetry (DSC) - (OECD 102)