Benzyl isovalerate

Boiling point

Link to relevant study record(s)

Reference

Endpoint:

boiling point

Type of information:

experimental study

Adequacy of study:

key study

Study period:

2017-01-12 – 2017-01-13

Reliability:

1 (reliable without restriction)

Rationale for reliability incl. deficiencies:

guideline study

Justification for type of information:

Experimental result performed using standard methods of analysis

Qualifier:

according to guideline

Guideline:

OECD Guideline 103 (Boiling Point)

Principles of method if other than guideline:

The boiling point determination of test item was done as per the test guideline OECD 103.

GLP compliance:

no

Type of method:

other: Siwoloboff

Key result

Boiling pt.:

215.6 °C

Atm. press.:

977.7 hPa

Remarks on result:

other: other details not available

Method Details	Observations	Remarks if, any
Guideline	OECD 103
Method	Method according to Siwoloboff
Principle of Boiling point test	A sample is heated gradually in a tube which is immersed in a liquid bath. The sample tube is held in close contact with a thermometer and it contains a boiling capillary which is fused about1 cm above its lower end. Upon approach of the boiling temperature bubbles emerge rapidly from the lower open end of the capillary. The boiling temperature is that temperature at which, on momentary cooling, the string of bubbles stops and liquid suddenly rises in the capillary.
Quantity of chemical used	g/ml	1 ml
Nature of the Bath taken	Oil bath Water bath	OIL
	If oil bath is used, specify Liquid paraffin Silicone oil	SILICON
Atmospheric pressure	hPa	977.7
mean Boiling point (°C) (RESULT)	°C	215.6

Conclusions:

The boiling point determination of test item was done following OECD Guideline 103 and according to the method of Siwoloboff. The test was conducted in replicates and mean boiling point was determined to be 215.6°C at 977.7 hPa.

Executive summary:

The boiling point determination of test item was done following OECD Guideline 103 and according to the method of Siwoloboff. The test was conducted in replicates and mean boiling point was determined to be 215.6°C at 977.7 hPa

Description of key information

The boiling point determination of test item was done following OECD Guideline 103 and according to the method of Siwoloboff. The test was conducted in replicates and mean boiling point was determined to be 215.6°C at 977.7 hPa

Key value for chemical safety assessment

Boiling point at 101 325 Pa:

215.6 °C

Additional information

The boiling point determination of test item was done following OECD Guideline 103 and according to the method of Siwoloboff. The test was conducted in replicates and mean boiling point was determined to be 215.6°C at 977.7 hPa

Other supporting studies from reliable sources such as authoritative database,review article and handbook suggests that he boiling point of chemical was reported to be in the range of 245 degree C to 246 degree C.

As the data from lab has K1 reliability and the test was performed using OECD guidelines which has the value of boiling point as 215.6 degree C ,thus considered as key study for the chemical safety assessment.