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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
28 September 2010 to 13 December 2010
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP Compliant, guideline study, available as unpublished report, acceptable with restrictions
Qualifier:
according to guideline
Guideline:
other: OECD 102/A1 Melting Freezing Temperature
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
other: Differential scanning calorimetry (DSC) using the procedure specified in ASTM E537-86
Decomposition:
yes
Decomp. temp.:
180 °C

Palladium (II) di(4 -oxopent-2 -en-2 -oate) decomposed from approximately 180 °C (453K), with no definitive signs of melting below 450 °C (723K).

Conclusions:
Palladium (II) di(4-oxopent-2-en-2-oate) decomposed from approximately 180 °C (453K), with no definitive signs of melting below 450 °C (723K).
Executive summary:

This is a GLP compliant, guideline study which is considered suitable for use as the key study for this endpoint. Palladium (II) di(4-oxopent-2-en-2-oate) decomposed from approximately 180 °C (453K), with no definitive signs of melting below 450 °C (723K).

Description of key information

Palladium (II) di(4-oxopent-2-en-2-oate) decomposed from approximately 180 °C, with no definitive signs of melting below 450 °C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
450 °C

Additional information

Walker and White (2011) is a GLP compliant, guideline study which is considered suitable for use as the key study for this endpoint. Palladium (II) di(4-oxopent-2-en-2-oate) decomposed from approximately 180 °C (453K), with no definitive signs of melting below 450 °C (723K).

The CRC handbook (Lide 2008) is a reliable peer reviewed handbook and so can be considered reliable and suitable for use as the supporting study for this endpoint. Palladium (II) 2,4 -pentanedioate decomposes before melting. The decomposition temperature is 205°C.