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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
01.09.2010
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2010

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
no
Other quality assurance:
ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Reference substance name:
1,4-Benzenedicarboxylic acid, 1,4-diisononyl ester
EC Number:
700-453-0
Cas Number:
59802-05-0
Molecular formula:
C26H42O4
IUPAC Name:
1,4-Benzenedicarboxylic acid, 1,4-diisononyl ester
Test material form:
liquid

Results and discussion

Melting / freezing point
Key result
Remarks on result:
not determinable

Any other information on results incl. tables

The sample was cooled to -150°C; rapidly for the first test, and controlled with a low cooling rate of -2 K/ min for the repeat measurement. Upon heating the heat flow curves of both tests show only a small glass transition at -86°C, indicating that the sample had solidified amorphously, regardless of cooling rate. No other thermal effect from crystallisation or melting was registered.

Applicant's summary and conclusion

Conclusions:
The melting temperature of the test item was determined by differential scanning calorimetry according to OECD guideline no. 102 (adopted on July 27, 1995) and EEC-Directive 92/69 EEC, Part A, Methods for the determination of physico-chemical properties, A.1 „Melting temperature"“, EEC Publication No. L383, December 1992
Melting point: no melting point.
Executive summary:

   extrapolated onset temperature [°C]  boiling temperature [°C] at 1013 hPa
 First run  359.10  358.86
 Second run  358.61  360.12
 Mean value    359.49