Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions
Remarks:
no GLP

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
no
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
m-(4,5-dihydro-5-imino-3-methyl-1H-pyrazol-1-yl)benzenesulphonic acid
EC Number:
268-387-0
EC Name:
m-(4,5-dihydro-5-imino-3-methyl-1H-pyrazol-1-yl)benzenesulphonic acid
Cas Number:
68083-38-5
Molecular formula:
C10H11N3O3S
IUPAC Name:
3-(5-imino-3-methyl-4,5-dihydro-1H-pyrazol-1-yl)benzene-1-sulfonic acid

Results and discussion

Melting / freezing point
Key result
Decomposition:
yes
Decomp. temp.:
340 °C
Remarks on result:
other: no melting point up to decomposition

Applicant's summary and conclusion

Conclusions:
The study was performed according to EU method A.1 with acceptable restrictions (no GLP) and therefore reliability of Klimisch 2 has been assigned. The substance decomposes at 340 °C without melting.
Executive summary:

The screening-DTA (closed glass crucible, heating rate 3 K/min, no GLP) of the sample Iminopyrazolsäure shows no melting point, but decomposes above about 340 °C with a heat release of about 180 kJ / kg. ‘Iminopyrazolsäure' exhibits no melting point up to 340 °C according to EC A.1.