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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
flash point, other
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experimental starting date: 14 August 2017 Experimental completion date: 18 September 2017
Reliability:
1 (reliable without restriction)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.9 (Flash-Point)
Deviations:
no
GLP compliance:
yes
Type of method:
closed cup
Flash point apparatus:
Setaflash apparatus

Test material

Constituent 1
Chemical structure
Reference substance name:
Oleic acid, compound with 2-amino-2-methylpropan-1-ol (1:1)
EC Number:
268-793-8
EC Name:
Oleic acid, compound with 2-amino-2-methylpropan-1-ol (1:1)
Cas Number:
68140-41-0
Molecular formula:
C18H34O2.C4H11NO
IUPAC Name:
oleic acid, compound with 2-amino-2-methylpropan-1-ol (1:1)
Specific details on test material used for the study:
Information as provided by the Sponsor. The Certificate of Analysis provided by the Sponsor is presented as Annex 1 (Please see the Attachment section of this Summary).

Identification: Oleic AMP
CAS No: 68140-41-0
Structure: Please see Illustration section below
Appearance/Physical state: Yellow paste
Batch: LAB4436
Purity: 100%
Expiry date: 21 February 2018
Storage conditions: Room temperature in the dark

Results and discussion

Flash point
Key result
Flash point:
127 °C
Atm. press.:
101.2 kPa

Any other information on results incl. tables

Results

Results of the flashpointdetermination are shown in the following table:

TestTemperature (ºC)

Observations

22.0

No flash.

27.0

No flash.

32.0

No flash.

37.0

No flash.

42.0

No flash.

47.0

No flash.

52.0

No flash.

57.0

No flash.

62.0

No flash.

67.0

No flash.

72.0

No flash.

72.0 (fresh sample)

No flash.

77.0

No flash.

82.0

No flash.

87.0

No flash.

92.0

No flash.

97.0

No flash.

102.0 (fresh sample)

No flash.

107.0

No flash.

112.0

No flash.

117.0

No flash.

122.0

No flash.

127.0

No flash, the test flame increased in size.

132.0

A blue flash spread across the sample cup.

132.0 (fresh sample)

A blue flash spread across the sample cup.

127.0 (fresh sample)

A blue flash spread across the sample cup.

122.0 (fresh sample)

No flash, the test flame increased in size.

123.0 (fresh sample)

No flash, the test flame increased in size.

124.0 (fresh sample)

No flash, the test flame increased in size.

125.0 (fresh sample)

No flash, the test flame increased in size.

126.0 (fresh sample)

No flash, the test flame increased in size.

127.0 (fresh sample)

A blue flash spread across the sample cup.

125.0 (fresh sample)

A blue flash spread across the sample cup.

Atmospheric pressure: 101.2 kPa
Observed flash point: 127.0°C
Corrected flash point: 127.0°C

Applicant's summary and conclusion

Conclusions:
The flash point of the test item has been determined to be 127 ± 2 °C.
Executive summary:

Thedeterminationwas carried out using a closed cup flash point tester*, using a procedure designed to be compatible with Method A.9 Flash Point of Commission Regulation (EC) No 440/2008 of 30 May 2008.

Apparatus:      Setaflash 30000-0 flash point tester


*Based on, Anon (1983) Paints, Varnishes, Petroleum and Related Products – Determination of Flash Point – Rapid Equilibrium Method,International Standard ISO 3679-2004 (E),Second Edition –2004-04-01,P1-18and Anon (1989) Flash Point of Liquids by Setaflash Closed-Cup Apparatus,ASTM D-3278-89,P1-7.

Conclusion

The flash point of the test item has been determined to be 127 ± 2 °C.

NOTE: Any of data in this dataset are disseminated by the European Union on a right-to-know basis and this is not a publication in the same sense as a book or an article in a journal. The right of ownership in any part of this information is reserved by the data owner(s). The use of this information for any other, e.g. commercial purpose is strictly reserved to the data owners and those persons or legal entities having paid the respective access fee for the intended purpose.