Reaction mass of Methylium, tris[4-(diethylamino)phenyl]- & acetate

Melting point / freezing point

Link to relevant study record(s)

Reference

Endpoint:

melting point/freezing point

Type of information:

experimental study

Adequacy of study:

key study

Study period:

12-03-2018 – 12-03-2018

Reliability:

1 (reliable without restriction)

Rationale for reliability incl. deficiencies:

guideline study

Justification for type of information:

Experimental test result performed using standard test guidelines

Qualifier:

according to guideline

Guideline:

other: As mention below

Principles of method if other than guideline:

The Freezing point determination of Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate was done using crushed ice and salt.

GLP compliance:

not specified

Type of method:

other: standard laboratory method

Specific details on test material used for the study:

- Name of the test material (IUPAC name): Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate- Common name: Basic Violet 4- Molecular weight: 515.7375- Molecular formula: C33H45N3O2- Smiles: CCN(CC)C1=CC=C(C=C1)C(=C2C=CC(=[N+](CC)CC)C=C2)C3=CC=C(C=C3)N(CC)CC.CC(=O)[O-]- Inchl: 1S/C31H42N3.C2H4O2/c1-7-32(8-2)28-19-13-25(14-20-28)31(26-15-21-29(22-16-26)33(9-3)10-4)27-17-23-30(24-18-27)34(11-5)12-6;1-2(3)4/h13-24H,7-12H2,1-6H3;1H3,(H,3,4)/q+1;/p-1- Substance type: Organic- Physical Appearance: greenish lustrous liquid- Stability: Stable in recommended storage conditions- Storage Conditions: Ambient Temp (23 to 27 °C)

Key result

Melting / freezing pt.:

< -8.6 °C

Atm. press.:

975 hPa

Decomposition:

no

Sublimation:

no

Remarks on result:

other: other details not available

Method	Freezing Temperature Method	Observations	Remarks if, any
Quantity of test item used	g	ml
Type of cooling bath used	Cold Water Crushed Ice Crushed Ice-Salt Dry Ice Other (specify)	Crushed Ice- Salt
Type and model no. of temperature sensor used	Glass thermometer Thermocouple Thermistor Other (specify)	Glass thermometer
Atmospheric pressure	hPa	971.4 hPa
Freezing point °C	°C	less than -12.4 °C

Conclusions:

The Freezing point of Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate was determined with freezing temperature and it was found to be less than -8.6 °C at 975 hPa.

Executive summary:

The Freezing point determination of Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate was done using crushed ice and salt. No freezing was observed up to -8.6°C.

Hence, the freezing point was inferred to be less than -8.6 °C at 975 hPa.

Description of key information

The Freezing point of Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetatee was determined with freezing temperature and it was found to be less than -8.6 °C at 975 hPa.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:

-8.6 °C

Additional information

The Freezing point determination of Reaction mass of Methylium, tris[4-​(diethylamino)​phenyl]​-​ & acetate was done using crushed ice and salt. No freezing was observed up to -8.6°C.

Hence, the freezing point was inferred to be less than -8.6 °C at 975 hPa.