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Physical & Chemical properties

Melting point / freezing point

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Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
comparable to guideline study with acceptable restrictions
Remarks:
Only one inweight with two heating intervals was conducted instead of at least two independent measurements. Company data: The results, the graphics and the SOPs for DSC and TGA measurements were available instead of a study report with a detailed description (materials, procedure, results, conclusion) of the measurement.
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
yes
Remarks:
only one inweight with two heating intervals was conducted instead of at least two measurements.
Qualifier:
equivalent or similar to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
yes
Remarks:
only one inweight with two heating intervals was conducted instead of at least two measurements.
Qualifier:
equivalent or similar to guideline
Guideline:
other: ISO 3146, DIN EN ISO 11357-1, DIN EN ISO 11357-2 (Draft)
Version / remarks:
SOPs according to the national standards
GLP compliance:
no
Type of method:
other: DSC, TGA/SDTA
Melting / freezing pt.:
>= 300 °C
Decomposition:
no
Sublimation:
no
Remarks on result:
other: DSC
Decomposition:
yes
Decomp. temp.:
>= 78 - <= 528 °C
Sublimation:
no
Remarks on result:
other: TGA

DSC

No observed melting up to 300 °C.

TGA

Phase 1: -0.63 % mass reduction up to 78 °C (Water)

Phase 2: -68.13 % mass reduction up to 528 °C (Disassociation)

Phase 3: -4.93 % mass reduction up to 760 °C (Unidentified)

Conclusions:
Potassium neodecanoate has no melting point up to 300 °C according to a DSC analysis. In a TGA a decomposition range from 78 °C up to 528 °C was recorded.

Description of key information

Potassium neodecanoate has no melting point up to 300 °C according to a DSC analysis. In a TGA a decomposition range from 78 °C up to 528 °C was recorded.

Key value for chemical safety assessment

Additional information