Registration Dossier

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
The study was conducted 13 February 2018 and 30 March 2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Other quality assurance:
ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
Reaction mass of 4,4'-methylenediphenol and 2,2'-methylenediphenol and o-[(4-hydroxyphenyl)methyl]phenol
EC Number:
908-912-9
Cas Number:
1333-16-0
Molecular formula:
C39H36O6
IUPAC Name:
Reaction mass of 4,4'-methylenediphenol and 2,2'-methylenediphenol and o-[(4-hydroxyphenyl)methyl]phenol
Test material form:
solid
Specific details on test material used for the study:
Sample name: supplied as a name of Bisphenol-F(Reaction mass of 2,2'-methylenediphenol and 4,4'-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)
Appearance: Solid
Purity: 98%
CAS: 1333-16-0

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
98.6 °C
Atm. press.:
101.3 kPa

Any other information on results incl. tables

Melting point of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]

Sample name

Item

Temperature

°C

K

Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]

Tm

98.6

371.8

Notes) Temperature in Kelvin (K) = Temperature in °C + 273.15

The sample was measured by differential scanning calorimeter (DSC)

Tm: melting temperature at 1stheating (peak maximum)

 

Results of DSC

Sample name

Item

Run

Temperature

Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]

Tm

°C

K

1

98.51

371.66

2

98.70

371.85

Average

98.61

371.76

Notes) Temperature in Kelvin (K) = Temperature in °C + 273.15

The sample was measured by differential scanning calorimeter (DSC)

Tm: melting temperature at 1st heating (peak maximum)

Applicant's summary and conclusion

Conclusions:
Melting temperature of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] was (98.6 ± 0.5) °C {(371.8 ± 0.5) K} at 101.3 kPa by DSC.
Executive summary:

The melting point of Bisphenol-F (Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] was measured by differential scanning calorimeter (DSC) using the procedure specified in Method 102 of the OECD Test Guidelines for Testing of Chemicals, 27 July 1995.

The results of the study were as follows:

Melting point of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]

Sample name

Item

Temperature

°C

K

Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)]

Tm

98.6

371.8

Notes) Temperature in Kelvin (K) = Temperature in °C + 273.15

The sample was measured by differential scanning calorimeter (DSC)

Tm: melting temperature at 1stheating (peak maximum)

 

Results of DSC

Sample name

Item

Run

Temperature

Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)

Tm

°C

K

1

98.51

371.66

2

98.70

371.85

Average

98.61

371.76

Notes) Temperature in Kelvin (K) = Temperature in °C + 273.15

The sample was measured by differential scanning calorimeter (DSC)

Tm: melting temperature at 1st heating (peak maximum)

 

Conclusion:

Melting temperature of Bisphenol-F(Reaction mass of 2,2’-methylenediphenol and 4,4’-methylenediphenol and 0-[(4-hydroxyphenyl)methyl]phenol)] was (98.6 ± 0.5) °C {(371.8 ± 0.5) K} at 101.3 kPa by DSC.