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Reaction products of diazotised Benzenesulfonic acid, 2-amino-5-[[2-(sulfooxy)ethyl]sulfonyl]-, subsequently coupled with Urea, N-(3-aminophenyl)-, subsequently condensation with 1,3,5-Triazine, 2,4,6-trichloro-, further condensation with Benzenesulfonic acid, 3-amino- and 3-Pyridinecarboxylic acid, sodium salts
EC number: 944-617-1 | CAS number: -
Particle size distribution (Granulometry)
Administrative data
Link to relevant study record(s)
- Endpoint:
- particle size distribution (granulometry)
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- From May 3, 2017 to June 16, 2017
- Reliability:
- 2 (reliable with restrictions)
- Rationale for reliability incl. deficiencies:
- guideline study with acceptable restrictions
- Qualifier:
- according to guideline
- Guideline:
- other: ISO 2926:2005 Aluminium oxide used for the production of primary aluminium-Particle size analysis for the range 45 μm to 150μm-Method using electroformed sieves
- Type of method:
- sieving
- Percentile:
- D50
- Mean:
- >= 100 - < 180 µm
- St. dev.:
- 0.028
- No.:
- #1
- Size:
- > 500 µm
- Distribution:
- 0.36 %
- No.:
- #2
- Size:
- >= 355 - <= 500 µm
- Distribution:
- 0.56 %
- No.:
- #3
- Size:
- >= 250 - <= 355 µm
- Distribution:
- 0.95 %
- No.:
- #4
- Size:
- >= 212 - <= 250 µm
- Distribution:
- 3.86 %
- No.:
- #5
- Size:
- >= 180 - <= 212 µm
- Distribution:
- 1.44 %
- No.:
- #6
- Size:
- >= 100 - <= 180 µm
- Distribution:
- 44.78 %
- No.:
- #7
- Size:
- >= 53 - <= 100 µm
- Distribution:
- 22.04 %
- No.:
- #8
- Size:
- < 53 µm
- Distribution:
- 25.34 %
- Conclusions:
- According to ISO 2926:2005, the mass fraction of particle sizes of CR SB07 were determined to be 0.36% in more than 500 μm particle size, 0.56% between 355 and 500 μm particle size, 0.95% between 250 and 355 μm particle size, 3.86% between 212 and 250 μm particle size, 1.44% between 180 and 212 μm particle size, 44.78% between 100 and 180 μm particle size, 22.04% between 53 and 100 μm particle size and 25.34% in less than 53 μm particle size.
The mass median diameter is 100 ~180 μm. - Executive summary:
This test using the procedures outlined in the ZCTC Study Plan for PCF2017-002 and ISO 2926:2005. With a sieve shaker, a certain mass of the sample is sieved through a series of sieves with various aperture size. Each mass of the separate fractions retained in the sieve is weighed and the mass distribution of the particle sizes could be calculated. The relative differences between the sum of all masses and the mass of the sample taken were both less than 1.5%. Therefore, all results were available. The mass fraction of particle sizes of CR SB07 were determined to be 0.36% in more than 500 μm particle size, 0.56% between 355 and 500 μm particle size, 0.95% between 250 and 355 μm particle size, 3.86% between 212 and 250 μm particle size, 1.44% between 180 and 212 μm particle size, 44.78% between 100 and 180 μm particle size, 22.04% between 53 and 100 μm particle size and 25.34% in less than 53 μm particle size.
Reference
Table 1. Determination results of the Particle size
No. |
1 |
2 |
Average value |
Mass of the sample (m0), g |
30.42 |
30.66 |
─ |
Mass of the residual on the sieve of 500 μm, g |
0.10 |
0.12 |
─ |
Mass fraction with more than 500 μm particle size, % |
0.33 |
0.39 |
0.36 |
Mass of the residual on the sieve of 355 μm, g |
0.16 |
0.18 |
─ |
Mass fraction with 355 μm - 500 μm particle size, % |
0.53 |
0.59 |
0.56 |
Mass of the residual on the sieve of 250 μm, g |
0.28 |
0.30 |
─ |
Mass fraction with 250 μm - 355 μm particle size, % |
0.92 |
0.98 |
0.95 |
Mass of the residual on the sieve of 212 μm, g |
1.19 |
1.17 |
─ |
Mass fraction with 212 μm - 250 μm particle size, % |
3.91 |
3.82 |
3.86 |
Mass of the residual on the sieve of 180 μm, g |
0.43 |
0.45 |
─ |
Mass fraction with 180 μm - 212 μm particle size, % |
1.41 |
1.47 |
1.44 |
Mass of the residual on the sieve of 100 μm, g |
13.65 |
13.70 |
─ |
Mass fraction with 100 μm - 180 μm particle size, % |
44.87 |
44.68 |
44.78 |
Mass of the residual on the sieve of 53 μm, g |
6.70 |
6.76 |
─ |
Mass fraction with 53 μm - 100 μm particle size, % |
22.02 |
22.05 |
22.04 |
Mass of the portion on the bottom reciver, g |
7.70 |
7.78 |
─ |
Mass fraction with less than 53 μm particle size, % |
25.31 |
25.38 |
25.34 |
Sum of all masses, g |
30.21 |
30.46 |
─ |
Relative difference (absolute value) between the sum and the mass of the sample taken, % |
0.69 |
0.65 |
─ |
Description of key information
The mass fraction of particle sizes of CR SB07 were determined to be 0.36% in more than 500 μm particle size, 0.56% between 355 and 500 μm particle size, 0.95% between 250 and 355 μm particle size, 3.86% between 212 and 250 μm particle size, 1.44% between 180 and 212 μm particle size, 44.78% between 100 and 180 μm particle size, 22.04% between 53 and 100 μm particle size and 25.34% in less than 53 μm particle size (ISO 2926:2005).
The mass median diameter is 100 ~180 μm.
Additional information
None.
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