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Diss Factsheets

Administrative data

Endpoint:
auto-ignition temperature (liquids)
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))
Deviations:
no
Qualifier:
according to guideline
Guideline:
DIN 51794 (Testing of mineral oil hydrocarbons - Determination of ignition temperature)
Deviations:
no
GLP compliance:
yes

Test material

Constituent 1
Chemical structure
Reference substance name:
N-methyldiallylamine
EC Number:
219-354-4
EC Name:
N-methyldiallylamine
Cas Number:
2424-01-3
Molecular formula:
C7H13N
IUPAC Name:
methylbis(prop-2-en-1-yl)amine
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: Lot 20160912
- Purity: 99.2%
- Expiration date of the lot/batch: 1-August-2018
STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: at room temperature
- Stability under test conditions: test substance stable

Results and discussion

Auto-ignition temperature (liquids / gases)
Key result
Auto-ignition temperature:
355 °C
Atm. press.:
>= 996 - <= 1 009 hPa

Any other information on results incl. tables

Table 1 Test Settings Main Study

 Test Volume (µL)

Start

Temperature (°C)

End

Temperature (°C)

 1

50 370 360 
 1 70 378 356
 1 90 373 371
 2 40 377 373
 2 60 367 353
 2 80 374 366 
 3 35 387 383
 3 65  370 360
 3 120 387 377

Table 2 Auto-ignition Temperature of MTDID 49220

 

 Test  Volume (µL)

Auto-ignition

Temperature

(°C)

Ignition

Delay

(seconds) 

Colour

of the

Flame

Minimum 

Auto-ignition

Temperature

(°C)

 1 50  362  11  orange/blue   358
 1 70 358 13 orange/blue  358
 1 90 373 13  orange/blue  358
 2 40 375 12 orange/blue  355
 2 60 355 12 orange/blue  355
 2 80 368 11 orange/blue

 355

 3 35 385 12 orange/blue  362
 3 65  362 12 orange/blue  362
 3 120 379 12 orange/blue  362

 

Applicant's summary and conclusion

Conclusions:
MTDID 49220 was determined to have an auto-flammability temperature of 355 °C, measured at atmospheric pressures of 996 and 1009 hPa, according to EU Method A.15.
Executive summary:

MTDID 49220 was determined to have an auto-flammability temperature of 355 °C, measured at atmospheric pressures of 996 and 1009 hPa. The study was conducted in accordance with EU Method A.15 and was GLP compliant; therefore the study is considered reliable without restrictions.

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