Registration Dossier

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
The study will be available 30th June 2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
yes
Type of method:
method to determine freezing temperature

Test material

Constituent 1
Chemical structure
Reference substance name:
Titanium 2,2',2''-nitrilotrisethanolate
EC Number:
240-015-1
EC Name:
Titanium 2,2',2''-nitrilotrisethanolate
Cas Number:
15879-01-3
Molecular formula:
C6H15NO3.xTi
IUPAC Name:
titanium 2,2',2''-nitrilotrisethanolate
Test material form:
liquid
Details on test material:
Test Item Name Tyzor TE
IUPAC Name titanium 2,2',2''-nitrilotrisethanolate
CAS No. 15879-01-3
EC No. 240-015-1
Appearance Light yellow liquid
manufactured by Dorf Ketal Speciality Catalyst Pvt Limited




Specific details on test material used for the study:
Test Item Name Tyzor TE
IUPAC Name titanium 2,2',2''-nitrilotrisethanolate
CAS No. 15879-01-3
EC No. 240-015-1
Batch number 334-300161/000004
Appearance Light yellow liquid
Manufactured by Dorf Ketal Speciality Catalyst Pvt Limited
Supplied to JRF by Dorf Ketal Speciality Catalyst Pvt Limited
Date of manufacture August 2017
Date of Expiry August 2019

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
ca. -42 °C
Decomposition:
no

Any other information on results incl. tables

Freezing Temperature of TYZOR TE

 

TABLE 1: Freezing Temperature of TYZOR TE

 

Replication-I

 

Bath Temperature
(° C)
Sample Temperature

(° C)

Complete Solidification

Observed

31
31
No
29
29
No
27
27
No
25
25
No
23
23
No
21
21
No
19
19
No
17
17
No
15
15
No
13
13
No
11
11
No
9
9
No
7
7
No
5
5
No
3
3
No
1
1
No
-1
-1
No
-3
-3
No
-5
-5
No
-7
-7
No
-9
-9
No
-11
-11
No
-13
-13
No
-15
-15
No
-17
-17
No
-19
-19
No
-21
-21
No
-23
-23
No
-25
-25
No
-27
-26
No
-29
-28
No
-31
-30
No
-33
-33
No
-35
-35
No
-37
-37
No
-39
-39
No
-41
-41
No
-43
-42
Yes


 

TABLE 1 (Continued)

 

Replication-II

 

Bath Temperature
(° C)
Sample Temperature
(° C)
Complete SolidificationObserved
0
0
No
-2
-2
No
-4
-3
No
-6
-5
No
-8
-8
No
-10
-10
No
-12
-12
No
-14
-14
No
-16
-16
No
-18
-18
No
-20
-20
No
-22
-23
No
-24
-25
No
-26
-26
No
-28
-28
No
-30
-29
No
-32
-32
No
-34
-34
No
-36
-36
No
-38
-38
No
-40
-40
No
-42
-42
Yes

 


 

TABLE 1 (Continued)

 

Replication-III

 

Bath Temperature
(° C)
Sample Temperature
(° C)
Complete Solidification Observed
0
0
No
-2
-2
No
-4
-3
No
-6
-6
No
-8
-8
No
-10
-10
No
-12
-12
No
-14
-14
No
-16
-16
No
-18
-18
No
-20
-20
No
-22
-22
No
-24
-25
No
-26
-26
No
-28
-28
No
-30
-29
No
-32
-32
No
-34
-34
No
-36
-36
No
-38
-38
No
-40
-40
No
-42
-42
Yes

 


 

Freezing Temperature of TYZOR TE

 

TABLE 2: Freezing Temperature of TYZOR TE

 

Replication

Freezing Temperature (°C)

R1

-42

R2

-42

R3

-42

Mean (°C)

-42

Standard Deviation

0.0


 

Applicant's summary and conclusion

Conclusions:
The mean Freezing Temperature of TYZOR TE was -42 ± 0.0 °C
Executive summary:

The Freezing Temperature of TYZOR TE was -42, -42, and -42 °C for replications R1, R2 and R3, respectively.

The mean Freezing Temperature of TYZOR TE was -42 ± 0.0 °C