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Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
November 15, 2017 – November 21, 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7220 (Boiling Point / Boiling Range)
Deviations:
no
GLP compliance:
yes
Type of method:
method according to Siwoloboff
Specific details on test material used for the study:
Composition: Reaction mass of dipotassium 3,3’-sulphonylbis(benzenesulphonate) and potassium 3-(phenylsulphonyl)benzenesulphonate
Purity: 92.8%
CAS# 63316-33-6 and 63316-43-8
Physical Description: White powder
Stability: Test substance was expected to be stable for the duration of testing.
Expiration Date: December 31, 2018
Key result
Decomposition:
yes
Remarks:
Color changed from white to light brown
Decomp. temp.:
289.5 °C

DECOMPOSITION POINT RESULTS

Replicate #

Decomposition Ranges Observed (°C)

Decomposition Point

Observed (°C)

Initial

Final

Individual

Mean ± SD

1

289.2

289.5

289.5

289.5± 0.0

2

289.2

289.5

289.5

Conclusions:
The substance decomposes at a temperature of 289.5 °C before boiling.
Executive summary:

In a GLP guideline study, the boiling point of the test substance was measured by the capillary technique using the Stuart SMP20 Melting Point Apparatus based on the procedures described in  OPPTS  830.7220, OECD TG 103, and EC method A2. This procedure was repeated with the test substance to obtain two measurements. The substance decomposes at a temperature of 289.5 °C before boiling as indicated by a color change from white to light brown.

Description of key information

In a GLP guideline study, the boiling point of the test substance was measured by the capillary technique using the Stuart SMP20 Melting Point Apparatus based on the procedures described in  OPPTS  830.7220, OECD TG 103, and EC method A2. This procedure was repeated with the test substance to obtain two measurements. The substance decomposes at a temperature of 289.5 °C before boiling as indicated by a color change from white to light brown.

Key value for chemical safety assessment

Additional information

The substance decomposes at a temperature of 289.5 °C before boiling as indicated by a color change from white to light brown.