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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
27 July 1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Other quality assurance:
ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Name:
CAS No.: Oleyl Lactate (Dermol OL)
42175-36-0 (formally known as)
EC NO:
Chemical Name

Physical state: 946-088-2 (assigned since pre-registration)
Reaction Products of (Z)-octadec-9-enol and lactic acid
Clear yellow liquid
Sponsor lot number: P7610
Purity: 100%
Molecular weight: 340.5405 g/mol
Arrival date: 7 February 2018
Re-test date: 31 January 2020
Storage conditions: Room temperature (15 to 30°C)
Boiling pt.:
225 °C
Atm. press.:
1 013 hPa
Conclusions:
A small exotherm from -50 to -35°C was observed, which would suggest solidification of a mixture (when a liquid is super cooled it may solidify when the temperature is increased). This was followed and endotherm from -33 to -2°C, which would suggest a mixture melting; this was confirmed by the freezing temperature test in this report, which was within this range

An exothermic artefact was recorded starting at 127°C, peaking at 225°C. A large exothermic reaction was observed to start at 333°C, which would be associated with decomposition. This was confirmed by a straw coloured liquid remaining in the crucible and a red stain on the outside of the lid.
Executive summary:

In this guideline (OECD 103) study, [conducted with GLP certification], A small exotherm from -50 to -35°C was observed, which would suggest solidification of a mixture (when a liquid is super cooled it may solidify when the temperature is increased). This was followed and endotherm from -33 to -2°C, which would suggest a mixture melting; this was confirmed by the freezing temperature test in this report, which was within this range

 

An exothermic artefact was recorded starting at 127°C, peaking at 225°C. A large exothermic reaction was observed to start at 333°C, which would be associated with decomposition. This was confirmed by a straw coloured liquid remaining in the crucible and a red stain on the outside of the lid.

Description of key information

Study conducted to recognised testing guidelines [with GLP certification].

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
225 °C

Additional information