Registration Dossier

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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
vapour pressure
Data waiving:
study scientifically not necessary / other information available
Justification for data waiving:
the study does not need to be conducted because the melting point is above 300°C
Justification for type of information:
JUSTIFICATION FOR DATA WAIVING
In TGA tests up to 1000°C it was observed that the substance actually does not melt at all.
Therefore the substance is expected to have a very low vapour pressure, which probaly would not be experimentally determinable.
Cross-reference
Reason / purpose for cross-reference:
data waiving: supporting information
Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
January 2018
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
comparable to guideline study with acceptable restrictions
Reason / purpose for cross-reference:
reference to same study
Qualifier:
no guideline followed
Principles of method if other than guideline:
TGA analysis was performed on 3 samples of the substance, up to 1000°C.
GLP compliance:
no
Type of method:
other: thermogravimetric analyses
Key result
Decomposition:
ambiguous
Decomp. temp.:
ca. 600 °C
Remarks on result:
not determinable

TGA curves of all 3 tested batches showed weight loss up to ca. 140 -150°C, and then an effect at approximately 600°C, which was ascribed to decomposition of residual OH and CO3 groups in the structure.

No distinct melting effect was observed, thus it is concluded that the substance has no melting temperature.

Conclusions:
The substance does not melt (up to 500°C).
Executive summary:

TGA analysis was performed on 3 batches of the substance, up to 1000°C. A dynamic rate high resolution program was used to obtain the data (Hi-Res sensitivity 1.0, Ramp 50.00°C/min, resolution 4.0).

Helium gas was used to create an inert atmosphere in all analyses.

In none of the tests a melting effect was observed. From this it is concluded that the substance does not have a melting point.

Data source

Materials and methods

Results and discussion

Applicant's summary and conclusion