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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Melting / freezing pt.:
-22.9 °C
Atm. press.:
ca. 101.3 kPa
Decomposition:
no
Sublimation:
no
Remarks on result:
other: result relates to glass transition temperature of the substance

In both experiment a glass transition was observed between -37 and -16°C on the heating curve. The extrapolated glass transition temperatures were -22.76 and -22.98°C in the initial and follow up experiments respectively. In both experiments, the sample had lost no mass and the consistency and colour of the sample had not changed.

Conclusions:
No endothermic peak corresponding to melting of the test substance was recorded in the tested temperature range from -50°C to 25°C. On both heating and cooling curves, a glass transition temperature of -22.9°C was determined.

Description of key information

No endothermic peak corresponding to melting of the test substance was recorded in the tested temperature range from -50°C to 25°C. On both heating and cooling curves, a glass transition temperature of -22.9°C was determined which is selected as the key value for chemical safety assessment.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-22.9 °C

Additional information