Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
The experimental start date was 14 May 2019, and the experimental completion date was 16 May 2019.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2019
Report date:
2019

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7220 (Boiling Point / Boiling Range)
Version / remarks:
Boiling Point/Boiling Range. August 1996.
Deviations:
yes
Remarks:
Melting or boiling, is indicated by a deviation from the base line in the heat flow record. Because melting and boiling are processes in which heat is consumed, the deviation from the base line is in the endothermic direction for these processes.
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
Boiling Point. July 27, 1995.
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: EC Guideline A.2.
Version / remarks:
Boiling Temperature. March 04, 2016.
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
(2S,3S)-2-benzhydryl-N-[(5-tert-butyl-2-methoxy-phenyl)methyl]quinuclidin-3-amine
EC Number:
831-973-7
Cas Number:
147116-67-4
Molecular formula:
C32H40N2O
IUPAC Name:
(2S,3S)-2-benzhydryl-N-[(5-tert-butyl-2-methoxy-phenyl)methyl]quinuclidin-3-amine
Test material form:
solid
Details on test material:
White to off-white powder.
Storage Conditions: At room temperature.

Results and discussion

Boiling point
Key result
Atm. press.:
ca. 101 325
Decomposition:
yes
Remarks:
(DSC) reaction and/or decomposition of the test item was observed starting at 325°C (598K)
Decomp. temp.:
>= 325
Remarks on result:
not determinable
Remarks:
Item has no boiling temperature, decomposition occurs.

Applicant's summary and conclusion

Conclusions:
Reaction and/or decomposition of the test item was observed during DSC experiments starting at 325°C (598K). Boiling of the test item was not observed below the temperature at which reaction and/or decomposition started. Based on this, the test item has no boiling temperature.

Executive summary:

Item has no boiling point, it decomposes.