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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
density
Remarks:
Density types indicated (migrated information): pour density; tap density
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: OECD guideline study, conducted to a high standard but not certified as being to GLP.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
GLP compliance:
no
Type of method:
other: Pour and tap densities for solids

Test material

Constituent 1
Chemical structure
Reference substance name:
1-hydroxy-2,2,6,6-tetramethylpiperidin-4-yl benzoate
EC Number:
807-702-3
Cas Number:
3225-26-1
Molecular formula:
C16H22NO3
IUPAC Name:
1-hydroxy-2,2,6,6-tetramethylpiperidin-4-yl benzoate
Test material form:
solid: crystalline
Details on test material:
- Material name: 4-hydroxyTEMPObenzoate
- Physical state: solid.
- Analysis date: 18th December 2014
- Analytical purity: 95.7 %.
- Impurities (identity and concentrations): triethylamine (0.56 %); 4-hydroxy TEMPO (0.8 %); deoxygenated benzoyl TEMPO (0.21 %); benzoic acid anhydride (1.48 %).
- Composition of test material, percentage of components: 95.7 % benzoyl TEMPO.
- Isomers composition: not applicable.
- Purity test date: 18 December 2014.
- Lot/batch No.: GP209
- Manufacturing date: 15/12/2014
- Expiration / re-test date of the lot/batch: 15/12/2015
- Stability under test conditions: stable.
- Storage condition of test material: Store in sealed container in cool dry place, away from heat and sunlight.

Results and discussion

Densityopen allclose all
Type:
pour density
Density:
0.4 g/L
Temp.:
20 °C
Type:
tap density
Density:
0.55 g/L
Temp.:
20 °C

Applicant's summary and conclusion

Executive summary:

The average pour density of benzoyl TEMPO is 0.400 g/mL

The average tap density of benzoyl TEMPO is 0.550 g/mL