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Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experiment start date - 06 November 2020; Experiment end date - 22 January 2021.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Identification: 4-Hydroxycoumarin
CAS Number: 1076-38-6
Appearance/Physical State: Beige powder
Batch Number: HCN20002
Purity: > 99%
Expiry Date: 26 September 2022
Storage Conditions: Room temperature, in the dark
Atm. press.:
1 atm
Decomposition:
yes
Decomp. temp.:
ca. 208 °C
Remarks on result:
not determinable
Remarks:
Decomposition was observed.
Conclusions:
The test item was determined to decompose from approximately 208 °C (481 K). As the test item decomposed, no value for the melting point could be determined.
Executive summary:

The melting point of the test substance was determined in a study conducted according to OECD Guideline 102 and Method A.1 . Differential scanning calorimetry was used for this purpose.

The test item was determined to decompose from approximately 208 °C (481 K). As the test item decomposed, no value for the melting point could be determined.

Description of key information

The melting point of the test substance was determined in a study conducted according to OECD Guideline 102 and Method A.1 . Differential scanning calorimetry was used for this purpose.

The test item was determined to decompose from approximately 208 °C (481 K). As the test item decomposed, no value for the melting point could be determined.

Key value for chemical safety assessment

Additional information