Registration Dossier
Registration Dossier
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EC number: 202-384-7 | CAS number: 95-02-3
Melting point / freezing point
Administrative data
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 29 April 2010 - 15 November 2010
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: GLP study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 010
- Report date:
- 2010
Materials and methods
Test guidelineopen allclose all
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.1 (Melting / Freezing Temperature)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Deviations:
- no
- GLP compliance:
- yes
- Type of method:
- capillary method
Test material
- Reference substance name:
- 4-amino-2-methylpyrimidine-5-methylamine
- EC Number:
- 202-384-7
- EC Name:
- 4-amino-2-methylpyrimidine-5-methylamine
- Cas Number:
- 95-02-3
- Molecular formula:
- C6H10N4
- IUPAC Name:
- 5-(aminomethyl)-2-methylpyrimidin-4-amine
- Details on test material:
- - Name of test material (as cited in study report): grewe-diamin
- Physical state: solid
Constituent 1
Results and discussion
Melting / freezing point
- Melting / freezing pt.:
- > 120 - < 129 °C
- Atm. press.:
- 1 atm
- Decomposition:
- no
- Sublimation:
- no
Applicant's summary and conclusion
- Conclusions:
- "Grewe-diamin" melted between 120 °C and 129 °C.
The difference between the temperature at the beginning and at the final stage of melting is not within the limits of the accuracy of the method
(+-0.5 °C) and therefore no melting point but a melting range was stated. The test substance melted in the range of 120 to 129 °C.
- Executive summary:
The determination of the melting temperature of the test substance was performed by the capillary method with hot block heating.
"Grewe-diamin" melted between 120 °C and 129 °C. The difference between the temperature at the beginning and at the final stage of melting is not within the limits of the accuracy of the method (+-0.5 °C) and therefore no melting point but a melting range was stated. The test substance melted in the range of 120 to 129 °C.
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