Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 202-384-7 | CAS number: 95-02-3
Boiling point
Administrative data
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 29 April 2010 - 15 November 2010
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: GLP-study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 010
- Report date:
- 2010
Materials and methods
Test guidelineopen allclose all
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling point/boiling range)
- Deviations:
- no
- GLP compliance:
- yes
- Type of method:
- method according to Siwoloboff
Test material
- Reference substance name:
- 4-amino-2-methylpyrimidine-5-methylamine
- EC Number:
- 202-384-7
- EC Name:
- 4-amino-2-methylpyrimidine-5-methylamine
- Cas Number:
- 95-02-3
- Molecular formula:
- C6H10N4
- IUPAC Name:
- 5-(aminomethyl)-2-methylpyrimidin-4-amine
- Details on test material:
- - Name of test material (as cited in study report): grewe-diamin
- Physical state: solid
Constituent 1
Results and discussion
Boiling point
- Atm. press.:
- 98.7 kPa
- Decomposition:
- yes
- Decomp. temp.:
- 190 °C
- Remarks on result:
- other: The decomposed test substance boiled from 295 °C on.
Any other information on results incl. tables
The test started at 130 °C. The colour of the test substance changed from yellowish to brown at 190 °C, to dark brown at 230 °C and to black at 265 °C. From 190 °C to 265 °C blistering not emerging the fused capillary was observed.
At about 295 °C the decomposed test substance started boiling and bubbles emerged rapidly from the lower open end of the capillary. Between 295 °C and 365 °C the test substance boiled but the capillary was not longer observable. At about 365 °C the test substance boiled over. Identical observations were made in both samples.
Applicant's summary and conclusion
- Conclusions:
- The test substance decomposed before boiling. Decomposition was indicated by a significant change of colour at 190 °C. The decomposed test
substance boiled from 295 °C on. - Executive summary:
The method of Siwoloboff was used.
The atmospheric pressure during the test was 98.7 kPa (calibrated barometer GPB 230, Petrotest, Germany).
The test substance decomposed before boiling. Decomposition was indicated by a significant change of colour at 190 °C. The decomposed test substance boiled from 295 °C on.
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
