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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
explosiveness
Type of information:
experimental study
Adequacy of study:
key study
Study period:
16.-18.02.2009
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP - Guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.14 (Explosive properties)
Deviations:
no
GLP compliance:
yes (incl. QA statement)

Test material

Constituent 1
Chemical structure
Reference substance name:
N-(4-{[3-(dimethylamino)propyl]sulfamoyl}phenyl)-2-[(2-methoxy-4-nitrophenyl)diazenyl]-3-oxobutanamide
EC Number:
700-222-4
Cas Number:
1065519-44-9
Molecular formula:
C22H28N6O7S
IUPAC Name:
N-(4-{[3-(dimethylamino)propyl]sulfamoyl}phenyl)-2-[(2-methoxy-4-nitrophenyl)diazenyl]-3-oxobutanamide
Details on test material:
- Name of test material (as cited in study report): 1003167-8200180-2149-1
- Physical state: yellow powder
- Analytical purity: no data
- Storage condition of test material: room temperature in the dark

Results and discussion

Small-scale preliminary testsopen allclose all
Parameter:
other: More sensitive to shock than m-dinitrobenzene
Remarks:
migrated information
Remarks on result:
other: no data
Remarks:
negative result in BAM fall hammer test
Parameter:
other: More sensitive to friction than m-dinitrobenzene
Remarks:
migrated information
Remarks on result:
other: no data
Remarks:
negative result in BAM friction test
Parameter:
other: Explosive under influence of flame
Remarks:
migrated information
Remarks on result:
negative (not further specified)
Remarks:
negative result in Koenen steel tube test

Any other information on results incl. tables

The test material has been determined not to have explosive properties.

BAM fall hammer test was done in 6 repetitions, in all there were no signs of ignition or explosion on impact. In 4 cases there were no signes of decomposition, in 2 cases when the test assembly was dismantled there were signs of decomposition: the material had tured a dark red colour.

BAM friction test was done in 6 repetitions, in all there were no signs of ignition or explosion and in all cases the dark red (or grey) mark on the porcelain plate and peg indicated decomposition.

Koenen steel tube test was done 3 times with 6mm Orifice Plate and 3 times with 2mm Orifice Plate and in all of the trials the tube was recovered intact.

Mean moisture content (from 2 determinations) was reported as 0.403 (% w/w)

Applicant's summary and conclusion