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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Qualifier:
equivalent or similar to guideline
Guideline:
other: OECD 104
Principles of method if other than guideline:
The determination of the Normal Boiling Temperature was performed by dynamic vapour pressure measurement according to OECD guideline 104
and 103 respectively.
GLP compliance:
yes (incl. QA statement)
Type of method:
dynamic method

Test material

Constituent 1
Chemical structure
Reference substance name:
bis(N,N,N-trimethyladamantan-1-aminium) sulfate
EC Number:
600-024-7
Cas Number:
1000777-61-6
Molecular formula:
C26 H48 N2 O4 S
IUPAC Name:
bis(N,N,N-trimethyladamantan-1-aminium) sulfate
Test material form:
other: granular
Details on test material:
Name of test material (as cited in study report): Tricyclo[3.3.1.13,7]decan-1-aminium, N,N,N,-trimethyl-, sulfate (2:1)
Analytical purity: 83.2 g/100g (by 1H NMR spectrometry; study no 11 L00496)
Lot/batch No.: ADTAS P5310.10.10
Expiration date of the lot/batch: Oct 20, 2011

Results and discussion

Boiling point
Boiling pt.:
> 350 °C
Atm. press.:
1 013 hPa
Remarks on result:
other: The upper temperature of the dynamic vapour pressure measurement is limited to 350°C by the equipment. Therefore the normal boiling temperature could not be determined.

Any other information on results incl. tables

Results:

The upper temperature of the dynamic vapour pressure measurement is limited to 350°C by the equipment. Therefore the normal boiling temperature could not be determined.

 Temperature [°C]  Vapour Pressure Measurement [hPa]
 > 350  1.01

Applicant's summary and conclusion