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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
30 March 2010-22 June 2010
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: This study has been performed according to OECD and EC guidelines and according to GLP principles.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2010

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
other: differential scanning calorimetry (DSC).

Test material

Constituent 1
Chemical structure
Reference substance name:
Ethyl 2-chloroacetoacetate
EC Number:
210-180-4
EC Name:
Ethyl 2-chloroacetoacetate
Cas Number:
609-15-4
Molecular formula:
C6H9ClO3
IUPAC Name:
ethyl 2-chloro-3-oxobutanoate
Details on test material:
- Name of test material (as cited in study report): Chloracetessigester
- Molecular formula: C6H9ClO3
- Molecular weight: 164.59
- Substance type: Clear slightly yellowish liquid
- Physical state: liquid
- Analytical purity: 93.9%
- Impurities (identity and concentrations): -
- Composition of test material, percentage of components: -
- Isomers composition: -
- Purity test date: -
- Lot/batch No.: 001008
- Expiration date of the lot/batch: 26 July 2010 (retest date)
- Stability under test conditions: Stable
- Storage condition of test material: At room temperature in the dark
- Other: -

Results and discussion

Melting / freezing point
Remarks on result:
other: Chloracetessigester has no melting temperature down to - 90°C.

Applicant's summary and conclusion

Conclusions:
The melting point was analyzed using differential scanning calorimetry (DSC). Chloracetessigester has no melting temperature down to - 90°C.