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Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
June 30, 2016 to August 16, 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point/Boiling Range)
Deviations:
no
GLP compliance:
yes
Remarks:
The study was conducted in compliance with the OECD Principles of GLP (1998).
Type of method:
method according to Siwoloboff
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: Dabeer S.A. (Batch/Lot No. 41401/1A0314)
- Expiration date of the lot/batch: 03/14/2019
- Purity test date: 03/15/2016

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: Storage in a cool, well ventilated place
Key result
Boiling pt.:
113.28 °C
Atm. press.:
760 mm Hg
Decomposition:
no
Remarks on result:
other: mean boiling point
Boiling pt.:
112.4 - 113.8 °C
Atm. press.:
760 mm Hg
Decomposition:
no

Replication Temperature of Initiation of Bubble Formation (°С) Temperature at which Continuous String of Bubbles were Observed (°С) Observed Boiling Point (°С) Boiling Range (°С) Boiling Point [in Kelvin (K)l Boiling Range (K)
Ri 103.12 113.62 113.62 112.42-113.8 388.77 385.57-388.77
R2 102.84 112.42 112.42 385.57
R3 102.66 113.81 113.81 386.96
Mean Boiling Point 113.28 - 387.10 -
Standard Deviation 0.75 - 1.6 -
Conclusions:
The mean boiling point was 113.28 °C.
Executive summary:

This study was performed to determine the boiling point / boiling range of HGA Ca (1:1) L according to OECD 103. The study was conducted in compliance with the OECD Principles of GLP (1998). The boiling point/boiling range was determined using Siwoloboff method. The experiment was carried out in three replications. The boiling range of HGA Ca (1:1) L was 112.42 -113.8 °С (385.57 - 388.77 K). The mean boiling point was 113.28 °C (± 0.75).

Description of key information

The boiling point/boiling point range of HGA Ca (1:1) L was determined using Siwoloboff method according to OECD 103 and GLP. The boiling point range was 112.42 -113.8 °С (385.57 - 388.77 K). The mean boiling point was 113.28 °C(± 0.75).

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
113.28 °C

Additional information

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