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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
03-04-2017 – 04-04-2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental result performed using standard methods of analysis
Qualifier:
according to guideline
Guideline:
other: as mentioned below
Principles of method if other than guideline:
The particle size distribution of test substance 2-methoxybenzoic acid was determined by Granulometric analysis with Rotap sieve shaker
GLP compliance:
no
Type of method:
sieving
Type of distribution:
counted distribution
Specific details on test material used for the study:
- Name of test material : 2-methoxybenzoic acid
- Molecular formula: C8H8O3
- Molecular weight : 152.1482 g/mol
- Smiles notation : COc1ccccc1C(=O)O
- InChl:1S/C8H8O3/c1-11-7-5-3-2-4-6(7)8(9)10/h2-5H,1H3,(H,9,10)
- Substance type:Organic
- Physical state:Solid
Key result
Percentile:
D50
Remarks on result:
other: no other details available
No.:
#1
Size:
150 µm
Distribution:
91.207 %
No.:
#2
Size:
106 µm
Distribution:
5.42 %
No.:
#3
Size:
75 µm
Distribution:
0.522 %
No.:
#4
Size:
53 µm
Distribution:
2.851 %

TEST METHOD: The particle size distribution was determined for test item o-anisic acid, CAS No 579-75-9.The test item is a alomost white odourless powder. (Colour and form of the chemical).The particle size distribution was determined with the help of Rotap sieve shaker. For this method,calibrated sieves were stacked with the coarsest opening sieve at the top of the stack and finest opening sieve at the bottom. 10.009 gm test item was weighed and put in the coarsest opening sieve placed at the top of the stack, covered with the lid. The stack was fitted in sieve shaker and was shaken for 10 minutes. The material was emptied from the above coarsest sieve into a pre-weighed petridishes. A soft bristle brush was used to

remove all the particles. The quantity obtained from the 1st sieves was weighed, and transferred to original apparatus. The above procedure was repeated for each sieve. Weight obtained from each sieve was then divided by the Test item quantity retained after sieving and percentage of each sieve was calculated

Conclusions:
The particle size distribution of chemical 2-methoxybenzoic acid (CAS No. 579-75-9 ) was determined by granulometric analysis with rotap sieve shaker. The particle size distribution was found to be in the range of 150 micron to 53micron.
Executive summary:

The particle size distribution of chemical 2-methoxybenzoic acid (CAS No. 579-75-9 ) was determined by granulometric analysis with rotap sieve shaker. The particle size distribution was found to be in the range of 150 micron to 53micron.

Description of key information

The particle size distribution of chemical 2-methoxybenzoic acid (CAS No. 579-75-9 ) was determined by granulometric analysis with rotap sieve shaker. The particle size distribution was found to be in the range of 150 micron to 53micron.

Additional information

The particle size distribution of chemical 2-methoxybenzoic acid (CAS No. 579-75-9 ) was determined by granulometric analysis with rotap sieve shaker. The particle size distribution was found to be in the range of 150 micron to 53micron.