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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2016-09-13 to 2016-12-08
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
May 2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
Version / remarks:
August 1996
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: ISO 1392
Version / remarks:
1977
Deviations:
no
GLP compliance:
no
Type of method:
method to determine freezing temperature
Key result
Melting / freezing pt.:
-15 °C
Atm. press.:
>= 988.8 - <= 991.8 mBar
Remarks on result:
other: result of 2 replicate measurements

A clear phase transition was observed at -15 °C. At the end of the measurement the test item was solid and white.

Conclusions:
The test item has a freezing temperature of -15°C.
Executive summary:

The freezing point of the test item was assessed according to OECD 102, with a crystallisation tube. The test item was cooled and a clear phase transition was observed at -15°C, which can be associated to the freezing of the test item. At the end of the measurement, the test item was solid and white.

Description of key information

For this endpoint, 1 study is available in which the freezing point was determined experimentally according to OECD 102, crystallisation tube method. The test item was found to freeze at a temperature -15°C. Additionally, a freezing point was reported in the CRC Handbook (1993): -15.05°C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-15 °C

Additional information

Freezing temperature.