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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
supporting study
Study period:
from 2017-08-28 to 2017-08-30
Reliability:
1 (reliable without restriction)
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
TOXI-COOP Toxicological Research Center Zrt., H-8230 Balatonfüred, Arácsi u. 97-99; Hungary (+ 5 further Hungarian addresses)
Type of method:
method to determine freezing temperature
Key result
Melting / freezing pt.:
< -29 °C
Atm. press.:
1 013.25 hPa
Decomposition:
no
Sublimation:
no

Table 1. Observations during the preliminary freezing point test

Temperature (°C)

Storage period

(hours)

State of the samples
Replicate 1 Replicate 2
-29 24 liquid liquid
-29 48 liquid liquid
Conclusions:
Based on the preliminary test, the freezing point of the test item is determined to be below -29 °C.
Executive summary:

A study was conducted according to OECD TG 102,Regulation (EC) No 440/2008method A.1 and guideline OPPTS 830.7200 to determine the freezing point of the test item. In the test the temperature of the phase transition from the liquid to the solid state was determined. As the test item was not frozen in the course of the preliminary test, the main test was not performed. According to Annex VII, point 7.2, column 2 of Regulation (EC) No. 1907/2006 the study does not need to be conducted below a lower limit of -20 °C. Based on the preliminary test, the freezing point of the test item was determined to be below -29 °C.

Endpoint:
melting point/freezing point
Data waiving:
study scientifically not necessary / other information available
Justification for data waiving:
other:

Description of key information

Based on the preliminary test, the freezing point of the test item was determined to be below -29 °C.

Key value for chemical safety assessment

Additional information

According to Annex VII, point 7.2, column 2 of Regulation (EC) No. 1907/2006 the study does not need to be conducted below a lower limit of -20 °C.

A supporting study was conducted according to OECD TG 102, Regulation (EC) No 440/2008 method A.1 and guideline OPPTS 830.7200 to determine the freezing point of the test item (references 4.2-2). In the test the temperature of the phase transition from the liquid to the solid state was determined. As the test item was not frozen in the course of the preliminary test, the main test was not performed. Based on the preliminary test, the freezing point of the test item was determined to be below -29 °C.