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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
February 09, 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Melting / freezing pt.:
ca. -28 °C
Remarks on result:
other: Extrapolated onset temperature

The extrapolated onset temperature was reported as -28°C, although the broad nature of the melting endotherm indicated that Reaction mass of morpholine and 6-[(p-tosyl)amino]hexanoic acid, compound with morpholine (1:1) melts over a temperature range. The results of the two experimental runs were in close agreement.

Conclusions:
An extrapolated onset temperature (i.e. melting point) of -28 °C was obtained for Reaction mass of morpholine and 6-[(p-tosyl)amino]hexanoic acid, compound with morpholine (1:1) following heating of the test material by differential scanning calorimetry
Executive summary:

The melting point of Reaction mass of morpholine and 6-[(p-tosyl)amino]hexanoic acid, compound with morpholine (1:1) was determined using differential scanning calorimetry, a thermosanalytical technique, in accordance with OECD Guideline 102 (Melting point / Melting Range). The extrapolated onset temperature of the melting of the substance was reported to be -28°C, although the broad nature of the melting endotherm suggested that the sample would melt over a temperature range. There was good correlation between either experimental run.

Description of key information

The extrapolated onset temperature of the melting of the substance was reported to be -28°C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-28 °C

Additional information