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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
The study was conducted 15 September 2016 to 23 May 2017.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
yes (incl. QA statement)
Remarks:
UK Department of Health, inspected 13 December 2016 certificate issued 15 March 2017
Type of method:
method according to Siwoloboff

Test material

Constituent 1
Reference substance name:
Fatty acids, vegetable-oil, polymd., unreacted fraction
EC Number:
273-100-7
EC Name:
Fatty acids, vegetable-oil, polymd., unreacted fraction
Cas Number:
68937-92-8
Molecular formula:
Substance is a UVCB - no structural or molecular formula is available.
IUPAC Name:
5-[(5E)-icos-5-enoyloxy]icosanoic acid
Specific details on test material used for the study:
Identity: RM1004951
Appearance: Clear yellow to amber liquid
Storage conditions: Room temperature (15 to 25°C)
Batch number: 1367Q13601
Purity: 100%
Expiry date: 17 September 2017
Date received: 05 October 2015

Results and discussion

Boiling point
Key result
Boiling pt.:
>= 173 °C
Atm. press.:
ca. 1 026 mBar
Decomposition:
yes
Decomp. temp.:
>= 173 °C

Any other information on results incl. tables

As the boiling tubes were heated at 1 degC/minute, the samples were observed to darken at temperatures above approximately 173°C, indicating decomposition. When heating was continued beyond this temperature in the preliminary trial, the sample continued to darken when heated to 360˚C where it did not boil.

Applicant's summary and conclusion

Conclusions:
It was not possible to determine the boiling temperature of the test substance as it decomposed at temperatures above approximately 173°C without boiling.
Executive summary:

It was not possible to determine the boiling temperature of the test substance as it decomposed at temperatures above approximately 173°C without boiling.