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Diss Factsheets

Administrative data

Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
17 Apr 2020
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2020
Report date:
2020

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.9 (Flash-Point)
Qualifier:
according to guideline
Guideline:
ISO 3679 (Determination of flash point - Rapid equilibrium closed cup method)
GLP compliance:
no
Other quality assurance:
ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
Type of method:
closed cup
Flash point apparatus:
other: Rapid tester

Test material

Constituent 1
Chemical structure
Reference substance name:
Reaction mass of 1,10-decanediol dimethacrylate (CAS 6701-13-9) and 10-methacryloyl-oxy-decylphosphate
Molecular formula:
C18H30O4 and C14H27O6P
IUPAC Name:
Reaction mass of 1,10-decanediol dimethacrylate (CAS 6701-13-9) and 10-methacryloyl-oxy-decylphosphate
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Batch number of test material: 5674800
- Purity: 91.8% (sum of two main components)
- Expiration date: 22 Jul 2020

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: Store in well-ventilated place. Keep container tightly closed. Store locked up.

Results and discussion

Flash point
Key result
Flash point:
183.5 °C
Atm. press.:
1 013 hPa
Remarks on result:
other: corrected to standard pressure

Any other information on results incl. tables

Amount of test item (g)   Temperature (°C)  Ignition (+/-)  Air pressure (hPa)
 3.99  174.0  -  988.6
 4.02  175.0  -  988.6
 4.33  176.0  -  988.6
 3.99  177.0  -  988.6
 4.02  178.0  -  988.6
 4.03  179.0  -  988.6
 4.13  180.0  -  988.6
 4.10  185.0  +  988.6
 4.17  184.0  +  988.6
 4.11  183.0  -  993.0
 4.03  183.0  -  933.0
 4.01  183.5  -  990.8
 4.21  183.5  +  990.8
 4.20  183.0  +  990.8
 4.05  182.5  -  990.8
 4.42  182.5  -  990.8
 4.11  182.5  -  990.8

An ignition is indicated by + and no ignition by -

Applicant's summary and conclusion

Conclusions:
The flash point for MDP was determined to be 183.5 °C at atmospheric standard pressure (EC A.9).
Executive summary:

The flash point of MDP was measured using a closed cup flash point apparatus. The study was tested starting at 174.0 °C, flame was applied at each 1 - 5 °C temperature rise, and then a second evolution of 0.5 °C between ignition points. Flash point was evaluated at an atmospheric pressure between 988.6 and 993.0 hPa and corrected to standard pressure. The study was conducted in accordance with regulation EC No. 440/2008 Method A.9. Flash Point and ISO guideline 3679. The study was conducted under the scope of the the laboratory's ISO/IEC 17025 certification. Therefore this study is considered reliable without restrictions.