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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
13 December 2011-16 March 2012
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Type of method:
thermal analysis
Remarks:
Differential scanning calorimetry.
Melting / freezing pt.:
15 °C
Atm. press.:
1 013 hPa

The sample shows an endothermic melting peak in the 12 to 25 °C region. The much smaller endothermic peak in the -26 to -11 °C region may be due to melting of minor components or processes occurring in the frozen sample.

Individual values:

Measurement       Onset       Peak

#1                     15.0 °C     20.6 °C

#2                     15.2 °C     20.7 °C

The mean onset is selected as giving the best value of the melting point. The difference between the lower onset value and the higher peak value is used to estimate the uncertainty.

Conclusions:
The melting point of the test substance is 15 ± 3 °C.
Executive summary:

The melting point of the test substance was determined according to the OECD Guideline 102 using differential scanning calorimetry. At 1013 hPa, the melting point is 15 +/- 3 °C.

Description of key information

The melting point of the test substance is 15 ± 3 °C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
15 °C

Additional information

The melting point of the test substance was determined according to the OECD Guideline 102 using differential scanning calorimetry. At 1013 hPa, the melting point is 15 +/- 3 °C.