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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
from 31 July 2018 to 06 September 2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with generally accepted scientific standards and described in sufficient detail

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guidelineopen allclose all
Qualifier:
equivalent or similar to guideline
Guideline:
EU Method A.9 (Flash-Point)
Version / remarks:
2016
Qualifier:
according to guideline
Guideline:
other: ASTM D7094: “Standard Test Method for Flash Point by Modified Continuously Closed Cup (MCCCFP) Tester”
Version / remarks:
2012
Deviations:
not specified
Qualifier:
according to guideline
Guideline:
ISO 3679 (Determination of flash point - Rapid equilibrium closed cup method)
Deviations:
not specified
Principles of method if other than guideline:
remark of reviewer:
Although ASTM D7094 (modified continuously closed cup) is not mentioned in the EC A.9 guideline, this method is a commonly used and safer (low sample volume) alternative for the ISO 2719 Pensky-Martens closed cup method.
GLP compliance:
yes
Type of method:
equilibrium method closed cup
Flash point apparatus:
other: Eraflash (Eralytics, Austria)
Dynamic viscosity of test material:
no data

Test material

Constituent 1
Chemical structure
Reference substance name:
Indene
EC Number:
202-393-6
EC Name:
Indene
Cas Number:
95-13-6
Molecular formula:
C9H8
IUPAC Name:
indene
Test material form:
liquid
Details on test material:
Appereance: Colorless transparent liquid
Storage conditions: At room temperature container flushed with nitrogen

Specific details on test material used for the study:
Boiling temperature: 181.5°C

Results and discussion

Flash point
Key result
Flash point:
58 °C
Atm. press.:
1 013 hPa

Any other information on results incl. tables

Modified continuously closed cup (ASTM D7094)

Test 1: 62°C

Test 2: 62°C

Flash point: 62°C

Rapid equilibrium method closed cup (ISO 3679)

Table: Equilibrium Method- Test with 5°C Interval

Test

Expected flash-point [°C]

Result

1

62

Flash

2

57

No flash

 

Table:  Equilibrium Method- Tests with 1°C Interval

Test

Expected flash-point [°C]

Result

1

58

Flash

Applicant's summary and conclusion

Interpretation of results:
Category 3 (flammable liquids) based on GHS criteria
Conclusions:
The flash point of the substance was determined to be 58°C (at 1013 hPa).
Executive summary:

The flash point of the substance was determined using the modified continuously closed cup ASTM D7094 method to be 62°C (at 1013 hPa).

Since the flash point was in the range of 60°C ± 2°C, the ISO 3679 rapid equilibrium closed cup method was also conducted. The flash-point of the substance was determined to be 58°C (at 1013 hPa).