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Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Version / remarks:
ISO 13320 -1 (2009)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 110 (Particle Size Distribution / Fibre Length and Diameter Distributions - Method A: Particle Size Distribution (effective hydrodynamic radius)
Deviations:
not specified
GLP compliance:
yes (incl. QA statement)
Other quality assurance:
other: QA unit
Type of method:
Laser scattering/diffraction
Type of particle tested:
other: wet small volume dispersion system used, several solvents tried to maximise dispersability
Remarks:
Silicone oil was selected as most suitable dispersant with minimum solubility
Type of distribution:
counted distribution

Test material

Constituent 1
Chemical structure
Reference substance name:
Bis[bis(3,5,5-trimethylhexyl)dithiocarbamate-S,S']zinc
EC Number:
283-381-8
EC Name:
Bis[bis(3,5,5-trimethylhexyl)dithiocarbamate-S,S']zinc
Cas Number:
84604-96-6
Molecular formula:
C38H76N2S4Zn
IUPAC Name:
bis({[bis(3,5,5-trimethylhexyl)carbamothioyl]sulfanyl})zinc
Test material form:
solid: particulate/powder
Specific details on test material used for the study:
BN 204873134010
Expiry - Aug 2015
White fine powder

Visual assessment
sample observed to be a fine white powder with clusters
At 400 x magnification under microscope, sample was made up of crystalline particles

Results and discussion

Mass median aerodynamic diameter:
ca. 25.55 µm
Geometric standard deviation:
ca. 2.2
Particle sizeopen allclose all
Key result
Percentile:
D50
Mean:
< 25.55 µm
St. dev.:
0.111
Remarks on result:
other: Std deviation of population
Key result
Percentile:
D90
Mean:
< 51.78 µm
St. dev.:
0.31
Remarks on result:
other: std devation of population
Key result
Percentile:
D10
Mean:
< 7.43 µm
St. dev.:
0.11
Remarks on result:
other: standard deviation of the population

Applicant's summary and conclusion