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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
9 - 12 Jun 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
not specified
GLP compliance:
yes
Type of method:
hot stages
Key result
Decomp. temp.:
135 °C
Remarks on result:
not determinable
Remarks:
decomposed at 135 C

Final Results:

There is no melting point of test item because the test item changed (decomposed) at about 135 °C.

 

Individual results:

Repetition #1

The test item was white powder before heating. The test item melted approximately 80% of its volume between about 135 °C and 140 °C, and then melted perfectly and fine bubbles were generated concurrently at about 205 °C. The contents in the sample tube were almost disappeared at about 215 °C.

 

Repetition #2

The test item was white powder before heating. The test item melted approximately 80% of its volume between about 135 °C and 140 °C, and then melted perfectly and fine bubbles were generated concurrently at about 200 °C. The contents in the sample tube were almost disappeared at about 215 °C.

 

Discussion:

It is considered that there is no melting point of the test item because the test item did not melt completely from about 135 °C to 140 °C. According to the information supplied by sponsor, the salts of perfluorocarboxylic acids are thermally decomposed. Therefore, the test item is considered to be decomposed at about 135 °C.

Description of key information

There is no melting point of test item because the test item changed (decomposed) at about 135 °C.

(OECD 102, hot stage).

Key value for chemical safety assessment

Additional information