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Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
26 November 2015 to 16 March 2016
Reliability:
1 (reliable without restriction)
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
other: Differential Scanning Calorimetry
Melting / freezing pt.:
-57.41 °C
Atm. press.:
1 019.6 hPa
Decomposition:
no
Sublimation:
no
Remarks on result:
other: Results of the DSC-measurement PN10184 Onset of endothermic effect
Melting / freezing pt.:
-57.06 °C
Atm. press.:
1 019.6 hPa
Decomposition:
no
Sublimation:
no
Remarks on result:
other: Result of DSC-measurement PN10185 Onset of endothermic effect

During the heating phase a distinct endothermic effect was observed in the temperature range of-70 – -40 °C, which can be associated with the melting of the test item. As the onset temperatures in both tests do not deviate by more than 0.5 K from their mean value of
-57.23 °C, this temperature can be used as freezing point. The test item has a melting point of -57.2 °C.

Conclusions:
The test item N,N-Dimethyloctan-1-amine has a melting point of -57.2 °C at atmospheric pressure (1013 hPa) as determined by differential scanning calorimetry according to Regulation EC No. 440/2008 Method A.1. and OECD Test Guideline 102 (1995).
Executive summary:

Report: Hernandez Carlota(2016): N,N-Dimethyloctan-1-amine Determination of physico-chemical properties Melting Point (EC A.1. and OECD 102) and Boiling Point (EC A.2. and OECD 103)

Source: consilab Gesellschaft für Anlagensicherheit mbH, Industriepark Höchst, G830/G840, 65926 Frankfurt am Main, Germany;

unpublished Report:CSL-15 -1314.05; Eurofins Study-No. S15 -06208

Guidelines: EC A.1. and OECD 102

Deviations: no

GLP: yes (incl. certificate)

Materials and Methods: Differential Scanning Calorimetry

Study period: 26 November 2015 to 16 March 2016

Results: The test item N,N-Dimethyloctan-1-amine has a melting point of -57.2 °C at atmospheric pressure (1013 hPa) as determined by differential scanning calorimetry according to Regulation EC No. 440/2008 Method A.1. and OECD Test Guideline 102 (1995).

Description of key information

The test item N,N-Dimethyloctan-1-amine has a melting point of -57.2 °C at atmospheric pressure (1013 hPa)

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-57.2 °C

Additional information