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Physical & Chemical properties

Density

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Reference
Endpoint:
tap density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
November 15, 2017 - November 21, 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7300 (Density / Relative Density / Bulk Density)
Deviations:
no
GLP compliance:
yes
Type of method:
pour and tap (for solids)
Specific details on test material used for the study:
Composition: Reaction mass of dipotassium 3,3’-sulphonylbis(benzenesulphonate) and potassium 3-(phenylsulphonyl)benzenesulphonate
Purity: 92.8%
CAS# 63316-33-6 and 63316-43-8
Physical Description: White powder
Stability: Test substance was expected to be stable for the duration of testing.
Expiration Date: December 31, 2018
Key result
Type:
tap density
Density:
0.782 g/cm³
Temp.:
20 °C
Key result
Type:
pour density
Density:
0.598 g/cm³
Temp.:
20 °C

MEASUREMENTS OF BULK DENSITY OF SOLIDS

 

Test Sample 1

Test Sample 2

Sample Weight (g)

26.6

26.8

Pour Volume (V1, mL)

0.1

0.1

Volume (V2, mL) after tap

26.5

26.7

Pour Density (g/mL)

0.602

0.593

Mean ± SD (g/mL)

0.598 ± 0.006

Tap Density (g/mL)

0.779

0.785

Mean ± SD (g/mL)

0.782 ± 0.004

Density in g/mL = Weight of sample divided by Volume (V1 or V2)

Conclusions:
The density of the test substance was determined to be 0.598 g/mL by the pour method and 0.782 g/mL by the tap method.
Executive summary:

In a GLP guideline study, the bulk density of the test substance was determined by the pour and tap methods based on the procedures described in  OPPTS  830.7300, OECD TG 109, and EC method A3 and found to be 0.598 g/mL and 0.782 g/mL, respectively.

Description of key information

In a GLP guideline study, the bulk density of the test substance was determined by the pour and tap methods based on the procedures described in  OPPTS  830.7300, OECD TG 109, and EC method A3 and found to be 0.598 g/mL and 0.782 g/mL, respectively.

Key value for chemical safety assessment

Additional information