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Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
12-Nov-2009 to 18-Nov-2009
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
- Purity: 99.72%
- Batch: not mentioned
Boiling pt.:
180.6 °C
Atm. press.:
1 013.3 hPa
Decomposition:
no

Two measurements in aluminium crucibles with a hole showed an endothermic effect after melting in the temperature range of 165-200°C with an onset temperature of approx. 180°C. The boiling point was corrected to standard atmospheric pressure (1013.3 hPa) = 180.6°C

 

Ident-No.

Onset / °C

Temperature range / °C

Crucible

29797

179.82

165-195°C

Aluminium with a hole

29796

180.61

165-200°C

Aluminium with a hole

 

.

Conclusions:
The boiling point was determined to be 180.6°C at 1013.3 hPa using the DSC-method.
Executive summary:

The measurement of the boiling point was performed in 2009 using the DSC-method at atmospheric pressure. The boiling point was found to be 180.6 °C at ca. 1013 hPa.

Description of key information

The boiling point was determined to be 180.6 °C at 1013 hPa, applying the DSC-method.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
180.6 °C

Additional information