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Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
January 2010
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
comparable to guideline study with acceptable restrictions
Qualifier:
equivalent or similar to guideline
Guideline:
other: DIN ISO 3016 / ASTM D97
GLP compliance:
no
Other quality assurance:
other: DIN EN ISO 9001
Type of method:
pour point
Remarks:
ISL Pourpoint CPP565
Key result
Melting / freezing pt.:
-77 °C
Atm. press.:
1 013 hPa
Remarks on result:
other: Pour point, mean of two replicate determinations

Two measurements were performed, with the following results:

-79 °C;

-75 °C;

giving a mean value of -77 °C for the pour point.

Conclusions:
Freezing Point (pour point; DIN ISO 3016 / ASTM D 97): - 77 °C
Executive summary:

The freezing point (pour point, determined similar / equivalent to DIN ISO 3016 / ASTM D 97) was determined to be -77 °C (mean of two replicate measurements: -79 °C; -75 °C).

The laboratory complied with a quality management system according to DIN EN ISO 9001 : 2008.

Description of key information

 Pour point (DIN ISO 3016 / ASTM D 97): -77 °C

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-77 °C

Additional information

The freezing point (pour point, determined similar / equivalent to DIN ISO 3016 / ASTM D 97) was determined to be -77 °C (mean of two replicate measurements: -79 °C; -75 °C).

The laboratory complied with a quality management system according to DIN EN ISO 9001 : 2008.